DOW 407 Diffusion Pump Fluid
Dow-704 Diffusion Pump Fluid
Sample: Dow 704 Diffusion Pump Fluid
Concentration: neat
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The following spectra were obtained on an EFT-60 spectrometer with
a 60 MHz magnet under standard operating parameters.
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1D proton spectrum
• data acquired and processed in about 11 seconds
• near integer values for the integrals
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Proton T1 via Inversion Recovery
• All data acquired and processed in about 3 minutes
• Automated data processing and stack plot via macro
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T1 Data reduction
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13C Spectrum
• Data acquired and processed in about 1 minute
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C13 T1 via Inversion Recovery
• All data acquired and processed in under 7 minutes
• Automated data processing and stack plot via macro
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DEPT Spectra
• Data acquired and processed in about 3 minutes.
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13C HETCOR Spectrum
• Data acquired and processed in less than ten minutes.
• Experiment used default values for acquisition parameters
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29Si XPT spectrum
• Data acquired and processed in < three minutes
• S/N = 74.0 using 32 scans
• Experimental value of JSiH ~20 Hz
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29Si 1-D spectrum
• Data acquired and processed in < three minutes
• S/N = 29.6 using 32 scans
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29Si HETCOR Spectrum
• Data acquired and processed in less than ten minutes.