Dow-704 Diffusion Pump Fluid
Sample: Dow 704 Diffusion Pump Fluid Concentration: neat

    
  • 1D proton spectrum

  • data acquired and processed in about 11 seconds

  • near integer values for the integrals

  • Proton T1 via Inversion Recovery

  • All data acquired and processed in about 3 minutes

  • Automated data processing and stack plot via macro


 
  • T1 Data reduction
  • 13C Spectrum

  • data acquired and processed in about 1 minute

  • C13 T1 via Inversion Recovery

  • All data acquired and processed in under 7 minutes

  • Automated data processing and stack plot via macro

 
  • DEPT Spectra – data acquired and processed in about 3 minutes.

 
  • 13C HETCOR Spectrum

  • data acquired and processed in less than ten minutes.

  • Experiment used default values for acquisition parameters

 

  • 29Si  XPT spectrum (top)

  • data acquired using the same parameters as 1D experiment

  • data acquired and processed in < three  minutes

  • S/N = 74.0 using 32 scans
     

  • 29Si  1-D spectrum (bottom)
  • data acquired and processed in < three  minutes

  • S/N = 29.6 using 32 scans

  • 29Si HETCOR Spectrum

  • data acquired and processed in less than ten minutes.

  • Experimental value of JSiH ~20 Hz